HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Methoxyphenylhydrazine hydrochloride → 3-Phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Methoxyphenylhydrazine hydrochloride | HCID 2723904 | — |
| Edukt | 2-(4-oxocyclohexyl)-2,3-dihydro-1H-isoindole-1,3-dione | HCID 11998391 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole | HCID 10807524 | 93,5% |
Reaktionsschritte
Reaction of 4-methoxyphenyl hydrazine hydrochloride (0.87 g, 5.0 mmol) with 4-phthalimido-cyclohexanone (1.22 g, 5.0 mmol) in ethanol (20 ml) heated under reflux for 2 hr, followed by cooling and removal of the precipitated solid by filtration gave 3-phthalimido-6-methoxy-1,2,3,4-tetrahydrocarbazole (1.62 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05464864 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-2fe2b57280cf4d178a630ea8ac6bf48e |
| Quellennotiz | uspto-grants-1995_11 |