HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Naphthol → Ethyl 6-(2-naphthyloxy)hexanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Naphthol | HCID 8663 | — |
| Edukt | Ethyl 6-bromohexanoate | HCID 117544 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Ethyl 6-(2-naphthyloxy)hexanoate | HCID 19375098 | — |
Reaktionsschritte
Ethyl 6-bromohexanoate and the sodium salt of 2-naphthol are reacted in DMF at 70° to provide ethyl 6-(2-naphthyloxy)hexanoate, which after the usual workup is reduced with lithium aluminum hydride in THF to provide 6-(2-naphthyloxy)hexanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05464865 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-cbe01735c94b4625940887766daee71c |
| Quellennotiz | uspto-grants-1995_11 |