Benzene → Phenylthionophosphonic dichloride

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.

Herkunft & Nachweise