HCID 18925402, Verbindung → HCID 18925414, Verbindung
Reaktionsgleichung
[N+](C1C=CSC=1C1C=CC(Cl)=CC=1)([O-])=O.[N+:16]([C:19]1[CH:23]=[CH:22][S:21][C:20]=1[C:24]1[CH:29]=[CH:28][C:27]([O:30][CH3:31])=[CH:26][CH:25]=1)([O-])=O>>[NH2:16][C:19]1[CH:23]=[CH:22][S:21][C:20]=1[C:24]1[CH:25]=[CH:26][C:27]([O:30][CH3:31])=[CH:28][CH:29]=1Komponenten
3
Versuchsvorschrift
The same procedures as described in Example 3 were carried out except that 3-nitro-2-(4-chlorophenyl)thiophene was replaced by 3-nitro-2-(4-methoxyphenyl)thiophene. The yield was 79%. 1 H-NMR(CDCl3, δ value):3.77(2H, brs), 3.83(3H, s), 6.65(1H, d, J=5.9), 6.96(2H, d, J=8.8), 7.07(1H, d, J=5.9), 7.43(2H, d, J=8.8)
Quellen und Nachweise
- ORD-Eintrag
- ord-abf48d0300384c768ac9010b1eaa4ddb
- Quelldatensatz
- uspto-grants-1998_05
- Patentnummer
- US05747518
Notizen zur Reaktion
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