HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine | HCID 70144893 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | cis-3-(3-(3-Hexenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 70144331 | — |
Reaktionsschritte
A mixture of methyl iodide (0,5 ml, 7.5 mmol) and cis-3-(3-(3-hexenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.9 g (46%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05750541 |
| Quelldatensatz | uspto-grants-1998_05 |
| ORD ID | ord-635f543bceef48a8ba806fbe0035889f |
| Quellennotiz | uspto-grants-1998_05 |