Methanol, 1,1-diethoxy-, 1-acetate → 6-Methyl[1,2,4]triazolo[1,5-a][1,3,5]triazine-7(6h)-thione

HRID 1289796

Reaktionsgleichung

Reaktionsgleichung von HRID 1289796
[NH2:1][C:2]1[N:6]([C:7]([NH:9][CH3:10])=[S:8])[N:5]=[CH:4][N:3]=1.[C:11](OC(OCC)OCC)(=O)C>>[CH3:10][N:9]1[C:7](=[S:8])[N:6]2[N:5]=[CH:4][N:3]=[C:2]2[N:1]=[CH:11]1

Komponenten

3

Edukt 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetateHCID 32648395-amino-N-methyl-1,2,4-triazole-1-carbothioamide

Produkt 1

HCID 2866546-Methyl[1,2,4]triazolo[1,5-a][1,3,5]triazine-7(6h)-thioneAusbeute 88 %

Versuchsvorschrift

The synthesis method of Example 55 was applied. The compound (1.49 g) obtained in Example 29 and diethoxymethyl acetate (12 ml) were used as reagents. The mixture was reacted at 75° C. for 2 hours to give 1.39 g of white crystals (yield 88%). The crystals were subjected to recrystallization from acetone to give white crystals.

Aufarbeitung

  1. customThe synthesis method of Example 55
  2. customThe mixture was reacted at 75° C. for 2 hours

Quellen und Nachweise

ORD-Eintrag
ord-4146b97b44e04cf2987c623a3440ef5f
Quelldatensatz
uspto-grants-1998_05
Patentnummer
US05750545

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