Methanol, 1,1-diethoxy-, 1-acetate → 2-[(Dimethylaminomethylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7(6H)-thione

HRID 1289798Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1289798
[NH2:1][C:2]1[N:6]([C:7]([NH:9][CH3:10])=[S:8])[N:5]=[C:4]([N:11]=[CH:12][N:13]([CH3:15])[CH3:14])[N:3]=1.[C:16](OC(OCC)OCC)(=O)C>>[CH3:15][N:13]([CH:12]=[N:11][C:4]1[N:3]=[C:2]2[N:1]=[CH:10][N:9]([CH3:16])[C:7](=[S:8])[N:6]2[N:5]=1)[CH3:14]

Komponenten

3

Edukt 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetateHCID 867525445-Amino-3-[(dimethylaminomethylidene)amino]-1-[methylamino(thiocarbonyl)]-1H-1,2,4-triazole

Produkt 1

HCID 867525462-[(Dimethylaminomethylidene)amino]-6-methyl-1,2,4-triazolo[1,5-a]-1,3,5-triazine-7(6H)-thioneAusbeute 56 %

Versuchsvorschrift

The synthesis method of Example 55 was applied. The compound (486 mg) obtained in Example 33 and diethoxymethyl acetate (5 ml) were used as reagents. The mixture was reacted at 95° C. for 2 hours to give 282 mg of pale-brown crystals (yield 56%).

Aufarbeitung

  1. customThe synthesis method of Example 55
  2. customThe mixture was reacted at 95° C. for 2 hours

Quellen und Nachweise

ORD-Eintrag
ord-691622487f6947b78fa0f9de9897e094
Quelldatensatz
uspto-grants-1998_05
Patentnummer
US05750545

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