Methanol, 1,1-diethoxy-, 1-acetate → HCID 10684276, Verbindung

Reaktionsgleichung

[NH2:1][C:2]1[N:6]([C:7]([NH:9][CH3:10])=[S:8])[N:5]=[C:4]([NH:11][C:12]([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[O:13])[N:3]=1.[C:19](OC(OCC)OCC)(=O)C>>[C:12]([NH:11][C:4]1[N:3]=[C:2]2[N:1]=[CH:10][N:9]([CH3:19])[C:7](=[S:8])[N:6]2[N:5]=1)([C:14]([O:16][CH2:17][CH3:18])=[O:15])=[O:13]

Komponenten

Edukt 2

HCID 84166Methanol, 1,1-diethoxy-, 1-acetate

HCID 86752547HCID 86752547, Verbindung

Produkt 1

HCID 10684276HCID 10684276, VerbindungAusbeute 78 %

Versuchsvorschrift

The synthesis method of Example 55 was applied. The compound (551 mg) obtained in Example 35 and diethoxymethyl acetate (8 ml) were used as reagents. The mixture was reacted at 90° C. for 2 hours to give 442 mg of white powdery crystals (yield 78%).

Aufarbeitung

customThe synthesis method of Example 55
customThe mixture was reacted at 90° C. for 2 hours

Quellen und Nachweise

ORD-Eintrag: ord-584e223ed1234dba9eb1c5f259aab9df
Quelldatensatz: uspto-grants-1998_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05750545

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