HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Butanaminium, N,N,N-tributyl-, azide → Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Butanaminium, N,N,N-tributyl-, azide | HCID 5743232 | — |
| Edukt | Ethanethioic acid cis-(+/-)-S-[tetrahydro-5-[[[(trifluoromethyl)-sulfonyl]oxy]methyl]-3-furanyl]ester | HCID 86750330 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | Ethanethioic acid cis-(+/-)-S-[5-(Azidomethyl)tetrahydro-3-furanyl]ester | HCID 86750331 | 87,8% |
Reaktionsschritte
The title compound is prepared by the procedure of Example 43 using 0.560 g of product from Example 60 in 2 ml of methylene chloride, 0.569 g of tetrabutylammonium azide in 2 ml of methylene chloride to give 0.321 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05750735 |
| Quelldatensatz | uspto-grants-1998_05 |
| ORD ID | ord-c12e3f1518d0405ca5678a752e817454 |
| Quellennotiz | uspto-grants-1998_05 |