HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → HCID 178508172, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | HCID 178478309 | HCID 178478309 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 178508172 | HCID 178508172 | — |
Reaktionsschritte
Using the method of Example 6, the product of Example 18, 0.2 g (0.0010 mole) of 4-chloro-1H-imidazo[4,5-c]quinoline was aminated at 175° C. in 12% ammonia in methanol to provide 1H-imidazo[4,5-c]quinolin-4-amine. The structure was verified by comparison of infrared and nuclear magnetic resonance spectra of the product with spectra of the product from Example 23.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05756747 |
| Quelldatensatz | uspto-grants-1998_05 |
| ORD ID | ord-9c4927f095e64bba899e764604c4df71 |
| Quellennotiz | uspto-grants-1998_05 |