HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Bromophenol | HCID 7808 | — |
| Edukt | Methyl vinyl ether | HCID 7861 | — |
| Produkt | p-Bromo-(1-methoxyethoxy)benzene | HCID 22908633 | 90% |
Reaktionsschritte
Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05468589 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-24808c6fb6474ee0bab5996c316c4c25 |
| Quellennotiz | uspto-grants-1995_11 |