HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Nitrophenethyl alcohol → 4-Aminophenethyl alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Nitrophenethyl alcohol | HCID 7494 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 4-Aminophenethyl alcohol | HCID 66904 | 87,7% |
Reaktionsschritte
A slurry of 5 g of 4-nitrophenethyl alcohol, 0.58 g of 10% Pd on carbon in 50 mL of absolute ethanol was shaken overnight under 50 psi of H2. The mixture was filtered and concentrated to yield 3.6 g of 4-(2-hydroxyethyl) aniline, mp 101°-102° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05468641 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-84bb3790b7794231954cde8825badf3b |
| Quellennotiz | uspto-grants-1995_11 |