HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Allyl Alcohol → Allyl 4-hydroxy-3-methoxybenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Allyl Alcohol | HCID 7858 | — |
| Edukt | Vanillic Acid | HCID 8468 | — |
| Lösungsmittel | Sulfuric Acid | HCID 1118 | — |
| Produkt | Allyl 4-hydroxy-3-methoxybenzoate | HCID 11117259 | 75% |
Reaktionsschritte
In a manner analogous to Example 1(a), 5 g (30 mmoles) of 4-hydroxy-3-methoxybenzoic acid treated at 100° C. for 4 hours with 50 ml of allyl alcohol and 820 μl of concentrated sulfuric acid, give 4.65 g (75% yield) of the expected ester in the form of a slightly yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05468897 |
| Quelldatensatz | uspto-grants-1995_11 |
| ORD ID | ord-877c07731dfd4847a8cf610d152a9e72 |
| Quellennotiz | uspto-grants-1995_11 |