Skatole → 1,2,7-trimethyl-1H-indole
Reaktionsgleichung
[CH3:1][C:2]1[NH:3][C:4]2[C:9]([CH:10]=1)=[CH:8][CH:7]=[CH:6][C:5]=2[CH3:11].[CH3:12]C1C2C(=CC=CC=2)NC=1>>[CH3:12][N:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][C:5]=2[CH3:11])[CH:10]=[C:2]1[CH3:1]Komponenten
3
Versuchsvorschrift
According to the procedure of Preparation 13 (a), except substituting 2,7-dimethylindole for the 3-methylindole, the title compound (960 mg, 87%) was obtained as an oil: MS (ES) m/e 160.2 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-1668f0b8d7534e1da500ebf6d2825c4d
- Quelldatensatz
- uspto-grants-2007_07
- Patentnummer
- US07250424B2
Notizen zur Reaktion
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