N-(3,4-Dichlorophenyl)thiourea → (3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	N-(3,4-Dichlorophenyl)thiourea	HCID 710776	—
Edukt	2-Bromo-4'-(methylsulfonyl)acetophenone	HCID 735823	—
Produkt	(3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine	HCID 32253410	78%

Reaktionsschritte

(3,4-Dichloro-phenyl)-[4-(4-methanesulfonyl-phenyl)-thiazol-2-yl]-amine was prepared in 78% yield using the procedure described in example 31 from 2-Bromo-1-(4-methanesulfonyl-phenyl)-ethanone and (3,4-Dichloro-phenyl)-thiourea. 1H NMR (300 MHz, DMSO-d6) δ 8.16-7.56 (m, 8H), 3.24 (s, 3H).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07381736B2
Quelldatensatz	uspto-grants-2008_06
ORD ID	ord-d8b297154fbb4023a7544f427b415052
Quellennotiz	uspto-grants-2008_06