HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pivalaldehyde → 3-(2,2-Dimethylpropylideneamino)-pyrrolidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pivalaldehyde | HCID 12417 | — |
| Edukt | 3-Aminopyrrolidine | HCID 164401 | — |
| Produkt | 3-(2,2-Dimethylpropylideneamino)-pyrrolidine | HCID 14836604 | — |
Reaktionsschritte
12.1 g (0.1 mol) of 71% strength pivalaldehyde, initially introduced into the reaction vessel and 8.6 g (0.1 mol) of 3-aminopyrrolidine are added dropwise at 20° C. to 30° C., while cooling in a water bath. The mixture is subsequently stirred at room temperature for 1 hour and is then distilled. Yield: 13.5 g (85% of theory), boiling point: 63° C.-65° C./10 to 12 mbar; content: 97%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05723627 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-8341607dd237492f8c1a68b89ed51a7c |
| Quellennotiz | uspto-grants-1998_03 |