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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 131665Erstellt: 25. Oktober 2026

3-Methyl-4-methoxybenzenamine → N-(4-Methoxy-3-methylphenyl)-2'-methyl-5'-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1'-biphenyl-4-carboxamide

https://huagongshe.com/reaction/131665

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Methyl-4-methoxybenzenamineHCID 67297—
Edukt2'-Methyl-5'-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1'-biphenyl-4-carbonyl chlorideHCID 21078801—
ProduktN-(4-Methoxy-3-methylphenyl)-2'-methyl-5'-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1'-biphenyl-4-carboxamideHCID 10273164—

Reaktionsschritte

N-(4-Methoxy-3-methylphenyl)-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carbonyl chloride and 4-methoxy-3-methylaniline using method K. NMR; δH [2H6]—DMSO 10.14,(1H, b), 8.05,(2H, d), 7.90,(1H, dd), 7.57-7.55,(5H, m), 6.92,(1H, d), 3.77,(3H, s), 2.57,(3H, s), 2.33,(3H, s), 2.16,(3H, s). LCMS; retention time 3.53 min, MH+ 414.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07384963B2
Quelldatensatzuspto-grants-2008_06
ORD IDord-d8e42392167f4c1797836b8a19abca60
Quellennotizuspto-grants-2008_06