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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 132089Erstellt: 25. Oktober 2026

Formic Acid → 1,2-Dodecanediol

https://huagongshe.com/reaction/132089

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktFormic AcidHCID 284—
EduktHydrogen PeroxideHCID 784—
Edukt1-DodeceneHCID 8183—
LösungsmittelEthanolHCID 702—
Produkt1,2-DodecanediolHCID 92866—

Reaktionsschritte

336 g (2.00 mol) of 1-dodecene were reacted with 236 g of formic acid and 185 g of a 50% strength aqueous H2O2 solution in accordance with Example 4. 412 g of ethanol were employed for the Marlon AS3 acid-catalyzed transesterification, and the main fraction obtained after the workup by distillation was 99.5% pure, virtually odorless 1,2-dodecanediol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07385092B2
Quelldatensatzuspto-grants-2008_06
ORD IDord-e3f2b7809e3f48e28f4d2541ab2247dc
Quellennotizuspto-grants-2008_06