HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(Phenylacetyl)-L-alanine → 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(Phenylacetyl)-L-alanine | HCID 7004640 | — |
| Edukt | 4-Aminoazepan-2-one | HCID 21584138 | — |
| Produkt | 3-(N'-(Phenylacetyl)-alaninyl)amino-epsilon-caprolactam | HCID 10215097 | — |
Reaktionsschritte
Following General Procedure B above using N-(phenylacetyl)-L-alanine (Example A) and 3-aminocaprolactam (Sigma), the title compound was prepared as a solid having a melting point of 200-202° C. The reaction was monitored by tlc on silica gel (Rf=0.30 in 1:9 methanol/dichloromethane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07390801B2 |
| Quelldatensatz | uspto-grants-2008_06 |
| ORD ID | ord-987c3041d8ff4f4fa979fdca053d055a |
| Quellennotiz | uspto-grants-2008_06 |