HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
L-Alanine ethyl ester → N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | L-Alanine ethyl ester | HCID 76507 | — |
| Edukt | Fluorophenylacetic acid | HCID 102649 | — |
| Produkt | N-[(2-phenyl)-2-fluoroacetyl]alanine Ethyl Ester | HCID 22894970 | — |
Reaktionsschritte
Following General Procedure BF above, and using α-fluorophenyl acetic acid (Aldrich) and alanine ethyl ester (Aldrich), the title compound was prepared. The reaction was monitored by tlc on silica gel (Rf=0.75 in 1:1 EtOAc:hexane) and purification was by chromatography on silica gel using 1:2 ethyl acetate/hexanes as the eluent.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07390801B2 |
| Quelldatensatz | uspto-grants-2008_06 |
| ORD ID | ord-8518db2c4b76423687970c4395dbf419 |
| Quellennotiz | uspto-grants-2008_06 |