4-Phenylpiperidine → 3-(4-Phenyl-1-piperidinyl)pyridine

Reaktionsgleichung

Ic1cccnc1.c1ccc(C2CCNCC2)cc1>CS(C)=O.Cc1cc(O)cc(C)c1NC(=O)C(=O)Nc1c(C)cc(O)cc1C.O=C([O-])[O-].[Cs+].[Cu][O][Cu]>c1ccc(C2CCN(c3cccnc3)CC2)cc1

customThe foil sealing tape was removed from the plate.
addition3 μL of a 0.0667 M solution of caffeine in DMSO was added to each reaction well using an SPT Labtech Mosquito® liquid handling robot
filtrationThe plates were then centrifuged for 15 to 20 seconds. · liquid-Phase beibehalten
aliquotFollowing centrifugation, 500 nL of the resultant mixture from each well was carefully dispensed into four 384-well analytical plates (Analytical Sales # 38435) using an SPT Labtech Mosquito® liquid handling robot. Each well of these analytical plates contained 30 μL of DMSO with 0.1% acetic acid, pre-dosed by OpenTrons, to facilitate analysis.

ORD-Eintrag: ord-ae8c0eb4431b4767bf3016099f3bd1df
Quelldatensatz: High-throughput exploration of 50,688 Pd-, Ni- and Cu-catalysed C–N coupling reactions
DOI: 10.1021/jacs.6c05959
Originallink: Quelle ansehen

Wird geladen…

customThe foil sealing tape was removed from the plate.
addition3 μL of a 0.0667 M solution of caffeine in DMSO was added to each reaction well using an SPT Labtech Mosquito® liquid handling robot
filtrationThe plates were then centrifuged for 15 to 20 seconds. · liquid-Phase beibehalten
aliquotFollowing centrifugation, 500 nL of the resultant mixture from each well was carefully dispensed into four 384-well analytical plates (Analytical Sales # 38435) using an SPT Labtech Mosquito® liquid handling robot. Each well of these analytical plates contained 30 μL of DMSO with 0.1% acetic acid, pre-dosed by OpenTrons, to facilitate analysis.

ORD-Eintrag: ord-ae8c0eb4431b4767bf3016099f3bd1df
Quelldatensatz: High-throughput exploration of 50,688 Pd-, Ni- and Cu-catalysed C–N coupling reactions
DOI: 10.1021/jacs.6c05959
Originallink: Quelle ansehen

Wird geladen…