HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Morpholine → 4-[2-(4-Nitrophenyl)ethyl]morpholine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Morpholine | HCID 8083 | — |
| Edukt | 4-Nitrophenethyl bromide | HCID 79266 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 4-[2-(4-Nitrophenyl)ethyl]morpholine | HCID 2797473 | — |
Reaktionsschritte
To 4-(2-bromoethyl)-1-nitrobenzene (1 eq) in tetrahydrofuran was added morpholine (3 eq) and stir for 16 h at ambient temperature. Concentrating and passing through a plug of silica gave 4-[2-(4-nitrophenyl)ethylmorpholine. MS: MH+=236.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728010B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-6a95f2b711a1461a8fd21c53214e6a68 |
| Quellennotiz | uspto-grants-2010_06 |