HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Amino-9-ethylcarbazole → (2S,4EZ)-4-(tert-butoxyimino)-1-(2-ethoxy-1-naphthoyl)-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Amino-9-ethylcarbazole | HCID 8588 | — |
| Edukt | 1-Naphthalenecarbonyl chloride, 2-ethoxy- | HCID 108679 | — |
| Edukt | (2S,4EZ)-1-(tertbutoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acid | HCID 131725425 | — |
| Produkt | (2S,4EZ)-4-(tert-butoxyimino)-1-(2-ethoxy-1-naphthoyl)-N-(9-ethyl-9H-carbazol-3-yl)-2-pyrrolidinecarboxamide | HCID 131725486 | — |
Reaktionsschritte
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(tert-butoxyimino)-2-pyrrolidinecarboxylic acid, 2-ethoxy-1-naphthoyl chloride, and 9-ethyl-9H-carbazol-3-amine the title compound was obtained in 47% purity by LC/MS. MS(ESI+): m/z=591.4.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07211601B2 |
| Quelldatensatz | uspto-grants-2007_05 |
| ORD ID | ord-49ba54081f96497a97adc21c6b2c92d8 |
| Quellennotiz | uspto-grants-2007_05 |