HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Phenethylamine → (2S)-2-methoxy-3-{4-[(1-Phenyl-ethylcarbamoyl)-methoxy]-phenyl}-propionic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Phenethylamine | HCID 7408 | — |
| Edukt | (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)propionic acid | HCID 9847886 | — |
| Edukt | (2S)-3-(4-carboxymethoxy-phenyl)-2-methoxy-propionic acid ethyl ester | HCID 58864673 | — |
| Produkt | (2S)-2-methoxy-3-{4-[(1-Phenyl-ethylcarbamoyl)-methoxy]-phenyl}-propionic acid | HCID 11725864 | — |
Reaktionsschritte
The title compound was prepared from (2S)-3-(4-carboxymethoxy-phenyl)-2-methoxy-propionic acid ethyl ester (PREPARATION 3, step 2) and 1-phenyl-ethylamine via the same procedure used for the preparation of (2S,1R)-2-ethoxy-3-(4-{1-[2-(4-phenoxy-phenyl)-ethylcarbamoyl]-ethoxy}-phenyl)-propionic acid (Example 1, step 3) to produce a colorless oil. MS (ES) for C20H23NO5 [M+H]+: 358.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07220880B2 |
| Quelldatensatz | uspto-grants-2007_05 |
| ORD ID | ord-fa4a817baaea4094bd5fa1a82fe86eba |
| Quellennotiz | uspto-grants-2007_05 |