HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → methyl (2S)-4-methyl-2-(methylamino)pentanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | 1,4-Dioxane | HCID 31275 | — |
| Edukt | N-Methylleucine | HCID 2777993 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | methyl (2S)-4-methyl-2-(methylamino)pentanoate | HCID 10921446 | 100% |
Reaktionsschritte
N-methyl-L-leucine (1.3 g, 8.95 mmol) was dissolved in 4M HCl, 1,4 dioxane (10 mL) and methanol (10 mL). The solution was stirred overnight at room temperature, then concentrated to afford the title compound as a white solid (100%). MS (ESI): 160.0 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06586466B2 |
| Quelldatensatz | uspto-grants-2003_07 |
| ORD ID | ord-c84cddade0974f8e87532868bc68310d |
| Quellennotiz | uspto-grants-2003_07 |