HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Carbonate → 3'-(N-Cinnamyl-N-methylaminomethyl)acetophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | N-methyl-3-phenylprop-2-en-1-amine | HCID 189183 | — |
| Edukt | 1-(3-(Bromomethyl)phenyl)ethan-1-one | HCID 15479807 | — |
| Edukt | N,6,6-trimethylhept-2-en-4-yn-1-amine | HCID 53427009 | — |
| Produkt | 3'-(N-Cinnamyl-N-methylaminomethyl)acetophenone | HCID 69936145 | 49,5% |
Reaktionsschritte
The procedure described in Example 1 was repeated, except that N-cinnamyl methylamine [instead of N-(6,6-dimethyl-2-hepten-4-ynyl)methylamine] (650 mg; 3.04 mmol), sodium carbonate (instead of potassium carbonate) (1.5 eq), and 3′-bromomethylacetophenone (1.5 eq) were used, to thereby yield 0.42 g of the target compound (yield: 49.5%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06586633B1 |
| Quelldatensatz | uspto-grants-2003_07 |
| ORD ID | ord-d8416139524347bfac9c50fba1398f58 |
| Quellennotiz | uspto-grants-2003_07 |