HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 2-(chloromethyl)-1,3-dimethoxyBenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | (2,6-Dimethoxyphenyl)methanol | HCID 2776839 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 2-(chloromethyl)-1,3-dimethoxyBenzene | HCID 12707002 | — |
Reaktionsschritte
0.43 g (2.56 mmol) of 2,6-dimethoxybenzyl alcohol was dissolved in 5 ml of benzene, and the resultant solution was added with 0.40 g (3.36 mmol) of thionyl chloride at a room temperature. The mixture was then stirred for an hour at a room temperature to facilitate the provided compounds to react. The reacted solution was then condensed under reduced pressure to obtain a crude product of 2,6-dimethoxybenzyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06589967B1 |
| Quelldatensatz | uspto-grants-2003_07 |
| ORD ID | ord-76f7ae5875dc448b82673af386701706 |
| Quellennotiz | uspto-grants-2003_07 |