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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1357029Erstellt: 26. Oktober 2026

Thionyl Chloride → 2-(chloromethyl)-1,3-dimethoxyBenzene

https://huagongshe.com/reaction/1357029

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktThionyl ChlorideHCID 24386—
Edukt(2,6-Dimethoxyphenyl)methanolHCID 2776839—
LösungsmittelBenzeneHCID 241—
Produkt2-(chloromethyl)-1,3-dimethoxyBenzeneHCID 12707002—

Reaktionsschritte

0.43 g (2.56 mmol) of 2,6-dimethoxybenzyl alcohol was dissolved in 5 ml of benzene, and the resultant solution was added with 0.40 g (3.36 mmol) of thionyl chloride at a room temperature. The mixture was then stirred for an hour at a room temperature to facilitate the provided compounds to react. The reacted solution was then condensed under reduced pressure to obtain a crude product of 2,6-dimethoxybenzyl chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06589967B1
Quelldatensatzuspto-grants-2003_07
ORD IDord-76f7ae5875dc448b82673af386701706
Quellennotizuspto-grants-2003_07