HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,1,3-Benzothiadiazol-5-ylmethanol | HCID 2776294 | — |
| Katalysator | HCID 178418406 | HCID 178418406 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 2,1,3-Benzothiadiazole-5-carbaldehyde | HCID 2776290 | 72,3% |
Reaktionsschritte
5-Hydroxymethylbenzo-2, 1,3-thiadiazole (2.6 g, 16 mmol) and manganese dioxide (6.0 g, 64 mmol) in chloroform (150 mL) were stirred at room temperature overnight. The reaction mixture was filtered off and the filtrate was evaporated to provide 1.9 g of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06593335B1 |
| Quelldatensatz | uspto-grants-2003_07 |
| ORD ID | ord-d6214540b07f41f691e40f83b9cf0f40 |
| Quellennotiz | uspto-grants-2003_07 |