HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isopropylamine → 2-Amino-N-isopropylbenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isopropylamine | HCID 6363 | — |
| Edukt | Isatoic Anhydride | HCID 8359 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-Amino-N-isopropylbenzamide | HCID 94411 | 77,1% |
Reaktionsschritte
A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07884098B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-7fc24b27a8664e549d66df96405fa8cf |
| Quellennotiz | uspto-grants-2011_02 |