Isopropylamine → 2-Amino-N-isopropylbenzamide

HRID 1362848

Reaktionsgleichung

Reaktionsgleichung von HRID 1362848
[C:1]12[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[NH:6]C(=O)[O:4][C:2]2=O.[CH:13]([NH2:16])([CH3:15])[CH3:14]>O>[NH2:6][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:1]=1[C:2]([NH:16][CH:13]([CH3:15])[CH3:14])=[O:4]

Komponenten

4

Edukt 2

HCID 6363IsopropylamineHCID 8359Isatoic Anhydride

Produkt 1

HCID 944112-Amino-N-isopropylbenzamideAusbeute 77,1 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid

Aufarbeitung

  1. customThe product precipitated from the reaction mixture
  2. filtrationthe reaction mixture was filtered
  3. washwashed with water

Quellen und Nachweise

ORD-Eintrag
ord-7fc24b27a8664e549d66df96405fa8cf
Quelldatensatz
uspto-grants-2011_02
Patentnummer
US07884098B2

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