HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
L-Tryptophan → L-(-)-Tryptophanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | L-Tryptophan | HCID 6305 | — |
| Lösungsmittel | Methan(2H)ol | HCID 123113 | — |
| Produkt | L-(-)-Tryptophanol | HCID 6951149 | 92% |
Reaktionsschritte
The title compound was prepared from (S)-tryptophan according to Method D and was isolated as a solid in 92% yield. δH (MeOD-d3) 7.46 (1H, d, J 7.9 Hz), 7.21 (1H, d, J 8.0 Hz), 6.96 (3H, m), 3.79 (1H, dd, J 11.3 and 3.6 Hz), 3.54 (1H, dd, J 11.3 and 6.2 Hz), 3.05 (1H, m), 2.80 (1H, m), 2.61 (1H, m). Note: exchangeable protons not evident in MeOD.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07888344B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-007bb295874144248d771a25b8014a86 |
| Quellennotiz | uspto-grants-2011_02 |