Cetyl Alcohol → Trolamine stearate

HRID 1364595

Reaktionsgleichung

C(OC[CH:16]([CH2:18][OH:19])O)(=O)CCCCCCCCCCC.[CH2:20]([OH:36])[CH2:21]CCCCCCCCCCCCCC.[C:37]([OH:56])(=[O:55])[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH3:54].CCCCCCCC[CH2:65][CH2:66][N+:67](CCCCCCCCCC)(C)C.[Cl-]>>[C:37]([OH:56])(=[O:55])[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH3:54].[N:67]([CH2:16][CH2:18][OH:19])([CH2:21][CH2:20][OH:36])[CH2:66][CH2:65][OH:55]

Komponenten

Edukt 4

HCID 2682Cetyl Alcohol2×

HCID 5281Stearic Acid

HCID 14871Monolaurin2×

HCID 23558Didecyldimethylammonium Chloride

Produkt 1

HCID 9867544Trolamine stearate

Versuchsvorschrift

Example 2A was repeated but for the sequence of addition of glycerol monolaurate and cetyl alcohol. Instead of being added in the second step, after the equimolar mixture of stearic acid and DDAC, the same amount of the glycerol monolaurate and cetyl alcohol added in Example 2 was added after the addition of TEA.

Aufarbeitung

additionInstead of being added in the second step
additionwas added
additionafter the addition of TEA

Quellen und Nachweise

ORD-Eintrag: ord-93ac90ce5ab0454ead1325f78ce482f1
Quelldatensatz: uspto-grants-2011_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07888393B2

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