HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Fluorophenol → (1R,2R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-(4-fluoro-phenoxymethyl)-cyclopentanecarboxylic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Fluorophenol | HCID 9732 | — |
| Edukt | (1R,2R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-hydroxymethyl-cyclopentanecarboxylic acid ethyl ester | HCID 59619451 | — |
| Produkt | (1R,2R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-(4-fluoro-phenoxymethyl)-cyclopentanecarboxylic acid ethyl ester | HCID 66919037 | — |
Reaktionsschritte
The title compound was prepared in analogy to example 68 step 5 using (1R,2R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-hydroxymethyl-cyclopentanecarboxylic acid ethyl ester (example 68 step 4) and 4-fluorophenol. Colorless oil (74%). MS (EI): 397.2 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07893099B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-9e0b5b62a35f4d3ba0d86c31311deb1b |
| Quellennotiz | uspto-grants-2011_02 |