HCID 18518556, Verbindung → HCID 18518619, Verbindung
Reaktionsgleichung
[CH2:1]([N:3]([CH2:22][CH3:23])[CH2:4][CH2:5][N:6]1[C:16]2[C:11](=[C:12]([C:18]([F:21])([F:20])[F:19])[CH:13]=[CH:14][C:15]=2[I:17])[C:9](=[O:10])[C:7]1=[O:8])[CH3:2].[CH:24]1[C:33]2[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=2)[CH:27]=[CH:26][C:25]=1[Mg]Br>>[CH2:22]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][N:6]1[C:16]2[C:11](=[C:12]([C:18]([F:20])([F:21])[F:19])[CH:13]=[CH:14][C:15]=2[I:17])[C:9]([OH:10])([C:26]2[CH:25]=[CH:24][C:33]3[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=3)[CH:27]=2)[C:7]1=[O:8])[CH3:23]Komponenten
3
Versuchsvorschrift
The title compound (103 mg, 53%) was prepared from 1-(2-diethylaminoethyl)-7-iodo-4-trifluoromethylisatin (152 mg, 0.345 mmol) and 2-naphthylmagnesium bromide by the procedure similar to that described in Example 1.
Quellen und Nachweise
- ORD-Eintrag
- ord-b4029a6aa0794ecebc4bd071cd229958
- Quelldatensatz
- uspto-grants-2003_06