Benzyl Bromide → N-[4-(allyloxy)benzyl]-N-benzyl-N-(2-methyl-3-nitrophenyl)amine
Reaktionsgleichung
[CH2:1]([O:4][C:5]1[CH:22]=[CH:21][C:8]([CH2:9][NH:10][C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[C:12]=2[CH3:20])=[CH:7][CH:6]=1)[CH:2]=[CH2:3].[CH2:23](Br)[C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH2:1]([O:4][C:5]1[CH:22]=[CH:21][C:8]([CH2:9][N:10]([CH2:23][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[C:12]=2[CH3:20])=[CH:7][CH:6]=1)[CH:2]=[CH2:3]Komponenten
3
Versuchsvorschrift
The product from Example 19A and benzyl bromide were processed as described in Example 6B to provide the title compound. MS (ESI+) m/z 389 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-df5bba0618c9409780a90df42b260d86
- Quelldatensatz
- uspto-grants-2003_06
- Patentnummer
- US06583180B2