1-(Bromomethyl)-2,4-difluorobenzene → N-{4-[3-(allyloxy)-5-methylphenoxy]benzyl}-N-(2,4-difluorobenzyl)-N-(2-methyl-3-nitrophenyl)amine
Reaktionsgleichung
[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:27]=[C:28]([CH3:30])[CH:29]=1)[O:8][C:9]1[CH:26]=[CH:25][C:12]([CH2:13][NH:14][C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([N+:21]([O-:23])=[O:22])[C:16]=2[CH3:24])=[CH:11][CH:10]=1)[CH:2]=[CH2:3].[F:31][C:32]1[CH:39]=[C:38]([F:40])[CH:37]=[CH:36][C:33]=1[CH2:34]Br>>[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:27]=[C:28]([CH3:30])[CH:29]=1)[O:8][C:9]1[CH:26]=[CH:25][C:12]([CH2:13][N:14]([CH2:34][C:33]2[CH:36]=[CH:37][C:38]([F:40])=[CH:39][C:32]=2[F:31])[C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([N+:21]([O-:23])=[O:22])[C:16]=2[CH3:24])=[CH:11][CH:10]=1)[CH:2]=[CH2:3]Komponenten
3
Versuchsvorschrift
The product from Example 89C and 2,4-difluorobenzyl bromide were processed as described in Example 6B to provide the title compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-6776fcba65fe41289fcdcfaf0a8fdec7
- Quelldatensatz
- uspto-grants-2003_06
- Patentnummer
- US06583180B2
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