HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Cyanophenyl isocyanate → N-(4-Cyanophenyl)-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Cyanophenyl isocyanate | HCID 170380 | — |
| Edukt | [4-(3,4-Dichlorobenzyl)morpholin-2-yl]methylamine | HCID 10308229 | — |
| Produkt | N-(4-Cyanophenyl)-N'-{[4-(3,4-dichlorobenzyl)morpholin-2-yl]methyl}urea | HCID 10136835 | 85,3% |
Reaktionsschritte
Example 25 was prepared in an analogous manner to Example 1 using a mixture of Intermediate 3 (0.025 g) and 4-isocyanatobenzonitrile (0.0196 g) to give the title compound (0.0325 g). LC-MS (System A): Rt 2.29 mins, Mass Spectrum m/z 419 [MH+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07157457B2 |
| Quelldatensatz | uspto-grants-2007_01 |
| ORD ID | ord-a89a76d8a64048c4977c8645b0c18244 |
| Quellennotiz | uspto-grants-2007_01 |