HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Pentanol → Amyl oleate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Pentanol | HCID 6276 | — |
| Edukt | Ethyl Oleate | HCID 5363269 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | Amyl oleate | HCID 5354230 | 91% |
Reaktionsschritte
A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728159B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-c891a9a360914f4b89c8c19dfb2ab01a |
| Quellennotiz | uspto-grants-2010_06 |