Reaktionsgleichung
C(CC(=O)C)(=[O:3])C.[H][H].[N:10]#[N:11].[O:12]=[O:13]>>[O:12]=[O:13].[N:10]#[N:11].[OH2:3].[N:10]#[N:11].[O:12]=[O+:13][O-:3].[N:10]#[N:11]Komponenten
Versuchsvorschrift
In the liquid phase method of manufacturing a phosphor from aqueous solution, organic metal salt or nitrate that contains elements composing the phosphor is dissolved in water, and then hydrolyzed to produce coprecipitation (hydrate) material. Here, the organic metal salt is alkoxide or acetylacetone, for example. The coprecipitation material is hydrothermally synthesized (crystallized in an autoclave), sintered in the air, or sprayed into a high temperature furnace, thereby obtaining powder. The powder is sintered for two hours at 1000 to 1400° C. in reducing atmosphere such as H2/N2=5/95 (%), crushed, and classified. Next, the resultant powder is sintered at 350 to 1000° C. in O2, O2—N2, H2O—N2, or O3—N2 to produce the phosphor.
Aufarbeitung
- customThe coprecipitation material is hydrothermally synthesized (
- customcrystallized in an autoclave), sintered in the air
- customobtaining powder
- customcrushed
Quellen und Nachweise
- ORD-Eintrag
- ord-debb0cbbe61a4ca7bf03fc55c305ffe1
- Quelldatensatz
- uspto-grants-2007_01
- Patentnummer
- US07161298B2
Verknüpfte Notizen
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