Hydrochloric Acid → Methyl 3-(sec-butylcarbamoyl)acrylate

HRID 1375214

Reaktionsgleichung

Reaktionsgleichung von HRID 1375214
[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([OH:12])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2].Cl.[CH3:14]O>>[CH:1]([NH:5][C:6]([CH:8]=[CH:9][C:10]([O:12][CH3:14])=[O:11])=[O:7])([CH2:3][CH3:4])[CH3:2]

Komponenten

4

Edukt 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 2445953-(Sec-butylcarbamoyl)acrylic acid

Produkt 1

HCID 54128810Methyl 3-(sec-butylcarbamoyl)acrylate

Versuchsvorschrift

To 3-(sec butylcarbamoyl)acrylic acid (20 g, 117 mmol) at room temperature was added 150 mL 1.2M HCl in methanol. The resulting mixture was stirred for two hours. Solvents were removed in vacuo to give the desired ester, which was used without further purification.

Aufarbeitung

  1. customSolvents were removed in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-5d1699450511463e996bfab6b995d881
Quelldatensatz
uspto-grants-2007_01
Patentnummer
US07166748B2

Verknüpfte Notizen

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