Methanol → Methyl 3,5-dichloro-4-methylbenzoate

Reaktionsgleichung

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([OH:7])=[O:6].[CH3:13]O>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Cl:12])[C:10]=1[CH3:11])[C:5]([O:7][CH3:13])=[O:6]

Komponenten

Edukt 2

HCID 887Methanol

HCID 185332343,5-Dichloro-4-methylbenzoic acid

Produkt 1

HCID 10130655Methyl 3,5-dichloro-4-methylbenzoate

Versuchsvorschrift

This compound was prepared in the same manner as in Reference Example 1 (step 1), except that 3,5-dichloro-4-methylbenzoic acid (Japanese Unexamined Patent Publication (Kokai) No. 6-192196) was used and methanol was used as the solvent, and that the crude product was purified by silica gel column chromatography.

Aufarbeitung

customthat the crude product was purified by silica gel column chromatography

Quellen und Nachweise

ORD-Eintrag: ord-e51b2b92542745ac848a958d9fc03db1
Quelldatensatz: uspto-grants-2010_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07728131B2

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