Methanol → HCID 21474555, Verbindung
Reaktionsgleichung
[CH3:1][OH:2].C(N(CC)CC)C.[C:10]([C:14]1[CH:15]=[C:16]([CH:30]=[CH:31][C:32]=1[O:33][CH3:34])[C:17]([O:19][CH2:20][C:21]1[CH:29]=[CH:28][C:24]([C:25](Cl)=[O:26])=[CH:23][CH:22]=1)=[O:18])([CH3:13])([CH3:12])[CH3:11]>C1COCC1>[C:10]([C:14]1[CH:15]=[C:16]([CH:30]=[CH:31][C:32]=1[O:33][CH3:34])[C:17]([O:19][CH2:20][C:21]1[CH:29]=[CH:28][C:24]([C:25]([O:2][CH3:1])=[O:26])=[CH:23][CH:22]=1)=[O:18])([CH3:13])([CH3:12])[CH3:11]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
5 ml of methanol, 460 μl of triethylamine and 50 ml of THF are introduced into a round-bottomed flask. A solution of 1.2 g (3.3 mmol) of 4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoyl chloride dissolved in 30 ml of THF is added dropwise and the mixture is stirred at room temperature for 4 h.