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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1378821Erstellt: 25. Oktober 2026

2-Isopropylaniline → 2,2'-Dithiobis[N-[2-(1-methylethyl)phenyl]benzamide]

https://huagongshe.com/reaction/1378821

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-IsopropylanilineHCID 12561—
Edukt2,2'-Dithiodibenzoyl chlorideHCID 88164—
LösungsmittelPyridineHCID 1049—
LösungsmittelDichloromethaneHCID 6344—
Produkt2,2'-Dithiobis[N-[2-(1-methylethyl)phenyl]benzamide]HCID 1893529314,3%

Reaktionsschritte

This compound was prepared according to the general method of Example 90 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 2-isopropylaniline (1.60 g, 11.6 mmol) in 13 mL of pyridine. The crude product was recrystallized twice from acetonitrile-DMF to yield 0.45 g of the title compound, mp 235°-237° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05668291
Quelldatensatzuspto-grants-1997_09
ORD IDord-178fffe81787489a90f7467744628364
Quellennotizuspto-grants-1997_09