Triethylamine → HCID 23323498, Verbindung

HRID 1381132Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1381132
[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]([NH2:15])=O)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].C(N(CC)CC)C>>[N+:1]([C:4]1[CH:5]=[C:6]([NH:10][C:11]2[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=2[C:13]#[N:15])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]

Komponenten

3

Edukt 2

HCID 8471TriethylamineHCID 54259173HCID 54259173, Verbindung

Produkt 1

HCID 23323498HCID 23323498, Verbindung

Versuchsvorschrift

3,85 g (15 mMol) of 2-(3-Nitrophenylamino)benzoic acid amide in 30 ml (0,325 Mol) phosphorooxychloride were treated with 4,32 ml (31 mMol) triethylamine which is added dropwise, whereby the reaction mixture warms up. After thirty minutes the excess of phosphorooxychloride is distilled off, the residue is treated with water and the solid product is filtered off.

Aufarbeitung

  1. additionis added dropwise
  2. distillationAfter thirty minutes the excess of phosphorooxychloride is distilled off
  3. additionthe residue is treated with water
  4. filtrationthe solid product is filtered off

Quellen und Nachweise

ORD-Eintrag
ord-9169ece5721a40f1a816b90af66ae9d8
Quelldatensatz
uspto-grants-1986_04
Patentnummer
US04585772

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