Hydrochloric Acid → HCID 178479216, Verbindung

HRID 1381351Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1381351
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793, Verbindung

Produkt 1

HCID 178479216HCID 178479216, Verbindung

Versuchsvorschrift

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

Aufarbeitung

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-43af6b268b6746e5b06c6e3873fd9716
Quelldatensatz
uspto-grants-1986_04
Patentnummer
US04585872

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