HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl 4-(1H-imidazol-1-yl)benzoate → N-[2-[Bis-(phenylmethyl)amino]ethyl]-4-(1H-imidazol-1-yl)-benzamide hemihydrate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl 4-(1H-imidazol-1-yl)benzoate | HCID 2766374 | — |
| Edukt | N1,N1-Dibenzylethane-1,2-diamine | HCID 6394114 | — |
| Produkt | N-[2-[Bis-(phenylmethyl)amino]ethyl]-4-(1H-imidazol-1-yl)-benzamide hemihydrate | HCID 67833593 | — |
Reaktionsschritte
Heat 4.23 g (21.0 mmol) of 4-(1H-imidazol-1-yl)benzoic acid methyl ester and 5.00 g (21.0 mmol) of N,N-dibenzylethylenediamine in 10 mL of xylenes at reflux for about 48 hr. Cool the solution to room temperature. Filter to obtain crystals of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04804662 |
| Quelldatensatz | uspto-grants-1989_02 |
| ORD ID | ord-c768e08e13ee4479b9ccd4c63185e2fa |
| Quellennotiz | uspto-grants-1989_02 |