HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1381992Erstellt: 26. Oktober 2026
Sulfuric Acid → 2,4-Dichloro-3-methyl-5-nitrobenzoic acid
https://huagongshe.com/reaction/1381992
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | Potassium Nitrate | HCID 24434 | — |
| Edukt | 2,4-Dichloro-3-methylbenzoic acid | HCID 13235951 | — |
| Produkt | 2,4-Dichloro-3-methyl-5-nitrobenzoic acid | HCID 13657443 | — |
Reaktionsschritte
30 g of 2,4-dichloro-3-methylbenzoic acid are initially introduced into 83 ml of concentrated H2SO4. 16.7 g of KNO3 are added in portions with ice cooling. The mixture is subsequently warmed at 50° C. for a further 2 hours and then poured onto ice. The nitro compound is isolated and recrystallized from toluene. Melting point 152°-4° C., yield: 24 g.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04804760 |
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| Quelldatensatz | uspto-grants-1989_02 |
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| ORD ID | ord-18b6946b2fdd45618207f6e8a407d1fb |
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| Quellennotiz | uspto-grants-1989_02 |
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