Ammonia → HCID 178472080, Verbindung

HRID 1382001Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1382001
[Cl:1][C:2]1[C:19]([N+:20]([O-:22])=[O:21])=[C:18]([Cl:23])[C:17]([F:24])=[CH:16][C:3]=1[C:4]([C:6](=[CH:12]OCC)[C:7]([O:9][CH2:10][CH3:11])=[O:8])=[O:5].[NH3:25]>C(O)C>[NH2:25][CH:12]=[C:6]([C:4](=[O:5])[C:3]1[CH:16]=[C:17]([F:24])[C:18]([Cl:23])=[C:19]([N+:20]([O-:22])=[O:21])[C:2]=1[Cl:1])[C:7]([O:9][CH2:10][CH3:11])=[O:8]

Komponenten

4

Edukt 2

HCID 222AmmoniaHCID 53944414Ethyl 2-(2,4-dichloro-5-fluoro-3-nitrobenzoyl)-3-ethoxyacrylate

Produkt 1

HCID 178472080HCID 178472080, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel2×

Versuchsvorschrift

38 g of the product from Example 1 are intitially introduced into 40 ml of ethanol. A mixture of 8 ml of concentrated NH3 solution in 25 ml of ethanol is added dropwise with ice cooling. The mixture is stirred for 2 hours at room temperature and the phases are then separated. The organic phase is washed with water and dried. 38.3 g of the title compound remain on concentration.

Aufarbeitung

  1. additionis added dropwise with ice cooling
  2. customthe phases are then separated
  3. washThe organic phase is washed with water
  4. customdried
  5. concentration38.3 g of the title compound remain on concentration

Quellen und Nachweise

ORD-Eintrag
ord-a0a1df0fb3fa461bad80ef8c291d42ba
Quelldatensatz
uspto-grants-1989_02
Patentnummer
US04804760

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