2-Methoxyaniline → Ethyl3-(2-methoxyphenylamino)acrylate
Reaktionsgleichung
[CH3:1][O:2][C:3]1[C:4]([NH2:9])=[CH:5][CH:6]=[CH:7][CH:8]=1.[C:10]([O:14][CH2:15][CH3:16])(=[O:13])[C:11]#[CH:12]>C(O)C>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][CH:12]=[CH:11][C:10]([O:14][CH2:15][CH3:16])=[O:13]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
o-Anisidine (57 ml, 0.5 mol) and ethyl propiolate (51 ml, 0.5 mol) were heated together under reflux in ethanol (200 ml) for 3 hours. The solvent was evaporated to afford ethyl 3-(2-methoxyphenylamino)acrylate as a yellow oil (55 g, 100%).
Aufarbeitung
- customThe solvent was evaporated
Quellen und Nachweise
- ORD-Eintrag
- ord-ea6efa9e52094d308d0c3e9bb06ac802
- Quelldatensatz
- uspto-grants-1989_02
- Patentnummer
- US04806549
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