HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzamide, N-cyano- → HCID 178512389, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzamide, N-cyano- | HCID 84805 | — |
| Edukt | 4-Amino-1-(2-naphthyl)methylpiperidine | HCID 11195823 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 178512389 | HCID 178512389 | 40,4% |
Reaktionsschritte
4-Amino-1-(naphth-2-ylmethyl)piperidine (1.0 g, 0.0042 m) and benzoyl cyanamide (0.67 g, 0.0042 m) in toluene (100 cm3) were refluxed for 15 hours. The solvent was evaporated and the residue recrystallised from the minimum amount of isopropyl alcohol and recrystallised twice more from ethanol to give 0.65 g of the title compound, m.p. dihydrochloride quarter hydrate, m.p. 260°-262° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04806552 |
| Quelldatensatz | uspto-grants-1989_02 |
| ORD ID | ord-8dae87f3430247cfba9c9f42b16f3681 |
| Quellennotiz | uspto-grants-1989_02 |